TOP

Equipment

The ultimate lab

Our department has different experimentation laboratories and techniques for obtaining, preparing and characterisation of materials

 

The materials can be obtained by chemical (chemical reactions), by means of ceramics (sintering) or by fusion at high temperatures.

 

We have a wide range of techniques of preparation and characterization in addition to the Institute of Ceramics and Glass (CSIC).

Furnaces

  • Gas Melting – 1500 ºC
  • Electrical Furnaces. Controlled Atmosphere – 1600 ºC
  • Electrical Tubular of Al2O3 – 1200 y 1600 ºC
    • Atmospheres N2, Ar, air
  • Electrical Tubular of Quartz – 1000 ºC
    • Atmospheres NH3, N2, Ar, air
    • Vaccum (10-3, 10-7 tor)
  • Electrical for ceramic tiles (50×50 cm) – 1300 ºC
  • Electrical mufle(1000 ºC)

 

Grinding, cutting, polishing

  • Planetary Moulin (agate, alumina) Fritsch
  • Moulin (agate)
  • Atrittion Moulin (alumina) for micromoulin
  • Turbula Mixer
  • Mixers for liquids and pastes (100 – 10000 rpm)
  • Micro – Cutting Isomet 4000
  • Polisher Buehler Beta

 

Spectroscopy

  • UV-vis (190 – 1100 nm). Perkin-Elmer Lambda 25 y Lambda 40
  • FT-IR (MIR: 4000 – 400 cm-1, with ATR module). Perkin-Elmer Spectrum BX
  • FT-IR (FIR: 4000 – 150 cm-1, with modules ATR, DRIFT and gas analysis). Nicolet 6700
  • Raman (Micro-Raman: 4000 – 100 cm-1, with modules Confocal and Heating Plate 0 – 600 ºC). Renishaw In Via.
  • Colorimeter Minolta
  • Brighness

 

Thermal Analysis

  • Thermogravimetric Analysis 10 – 1500 ºC. Perkin-Elmer Pyris 1 TGA
  • Differential Thermal Analysis 10 – 1500 ºC. Perkin-Elmer DTA 7
  • Simultaneous Thermal Analysis DTA-TG-DSC (10 – 1500 ºC) with gas analysis by FT-IR. SDT Q 600

 

Elemental Analysis

  • Carbon – Sulfur. Leco CS 200
  • Nitrogen – Oxygen. Leco TC500
  • Carbon, Hydrogen (water). Leco RC 412

 

Porosity, density

  • Nitrogen Adsorption 77 K. Micromeritics Tristar 3000
  • He Pycnometry (Micromeritics AccuPyc 1330, Quantachrome MicroPycnometer)
  • Densimetry of plastics

 

Chromatography

  • Gas Chromatographs with Flame Ionization Deterctors (Perkin Elmer: Autosystem, Calrius 580)

 

Optical microscopy, refraction index, polaroscopy

  • Matalographic Microscope (2.5, 5, 20, 50 y 100 aumentos). Leika DM LM
  • Transmission Microscope (2 -63 aumentos). Leika DK 1000
  • Lupa binocular Leica L2
  • Refraction Index Abbe. Atago
  • Polariscope Sharples UK

 

  Misc

  • RTM equipment for fiber reinforced composites – poliester
  • Glass-Glass and Glass-Metal Solding
  • 3D ceramic digital printing. Z Printer 310 Plus
  • Viscosimetries (Fungilab and Visco Star Plus)
  • Ice Camera. Dycometal CET
  • Climatic Cameras H2O, SO2 y UV (Dycometal VCK 30, AFA 288, B)
  • Centrifugadora Nüve NF800
  • Liofilizador Alpha 1-4 LD
  • Ovens of forced air, vaccum, etc.
  • Rotavapor Lab 4000
  • Heating plates
  • pH-meter
  • Oximeter
  • Conductimeter

 

Surfaces Processes Advanced Ceramics Glass